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Of course, the following methods are to measure the original mass in the sample, and then fully heat it to see how much the mass is reduced, and what is reduced is the H2O and CO2 released in 2NaHCO3=Na2CO3+H2O+CO2, so that the mass of NaHCO3 in it is known, and finally of course it must be converted into the original sample mass.
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Determination method of sodium carbonate:
Take a sample (a certain volume of sample solution V), add phenolphthalein as an indicator, titrate with hydrochloric acid standard solution C(HCl) (mol L) until the red color disappears, and note the volume of hydrochloric acid used (V1).At this point, NaOH has been completely neutralized, and Na2CO3 has been neutralized to NaHCO3Then use methyl orange as an indicator to continue titration with hydrochloric acid standard solution to orange (in order to make the observation endpoint obvious, the titration can be paused before the endpoint and the CO2 can be removed by heating), and the volume of hydrochloric acid used (V2) is noted
V2 is the volume of hydrochloric acid consumed to titrate NaHCO3.
Determination method of C(Na2CO3)=C(HCl)*V2 VC(NaOH)=(V1-V2)*C(HCl)V sodium bicarbonate:
Add acid to generate carbon dioxide, and then use the drainage method to obtain the volume of carbon dioxide, carbon dioxide mol can calculate the amount of carbon dioxide, and then indirectly obtain the amount of baking soda, and find the mass of sodium bicarbonate can calculate its content.
Not sure if you're measuring sodium carbonate or sodium bicarbonate. )
The selection of indicators is related to the nature and state of the reactants.
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The methods for distinguishing sodium carbonate solution from sodium bicarbonate solution include gas method, precipitation method and pH measurement method. You can take an appropriate amount of two solutions to be identified, and after adding a small amount of hydrochloric acid, the sodium bicarbonate solution that can immediately produce bubbles, and the sodium carbonate solution that produces bubbles more slowly.
Gas delay and dry merger method: take an appropriate amount of two solutions to be identified, add a small amount of hydrochloric acid, and immediately produce bubbles of sodium bicarbonate solution. The slower to produce bubbles is the sodium carbonate solution.
Precipitation method: take an appropriate amount of two solutions to be identified, add an appropriate amount of barium chloride solution or calcium chloride solution, and the sodium carbonate solution that can produce precipitation is the sodium carbonate solution.
pH measurement: use pH to measure the dilute solution of the same concentration, and the larger pH is the sodium carbonate solution.
Observation: Both are white in the solid state. Sodium carbonate is observed to be powdery in appearance and sodium bicarbonate in crystalline form.
Heating method: after heating, it is sodium bicarbonate that can produce the gas that makes the clarified lime water turbid, and vice versa; Before and after heating, it is called its mass, and the one whose mass has decreased is sodium bicarbonate, and vice versa.
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Summary. 1. The safe dosage is between. 2. Baking soda generally refers to sodium bicarbonate, white crystalline powder.
It is odorless, alkaline, and easily soluble in water. It slowly decomposes in moist or hot air to produce carbon dioxide, which is heated to 270 and loses all carbon dioxide. In case of acid, it decomposes strongly to produce carbon dioxide.
3. Sodium ions are the normal needs of the human body and are generally considered non-toxic. However, excessive ingestion may cause alkalosis. Sodium bicarbonate solids begin to gradually decompose above 50 to form sodium carbonate, water and carbon dioxide gas, and this property is often used as a leavening agent for making biscuits, pastries, steamed bread and bread.
Sodium bicarbonate will remain sodium carbonate after action, and too much use will make the finished product have an alkaline taste.
1. The safe dosage is destroyed in between. 2. Baking soda generally refers to sodium bicarbonate, white crystalline powder. It is odorless, alkaline, and easily soluble in water.
It slowly decomposes in moist or hot air to produce carbon dioxide, which is heated to 270 and loses all carbon dioxide. In case of acid, it decomposes strongly to produce carbon dioxide. 3. Sodium ions are the normal needs of the human body and are generally considered non-toxic.
However, excessive ingestion may cause alkalosis. Sodium bicarbonate solids above 50 begin to gradually decompose to produce sodium carbonate, water and carbon oxide gas in the second mold, which is often used as a leavening agent for making biscuits, cakes, steamed bread and bread. Sodium bicarbonate will remain sodium carbonate after action, and too much use will make the finished product have an alkaline taste.
How to detect the moisture content of sodium bicarbonate?
You are wrong! I'm asking how much of the moisture content of sodium bicarbonate is within the normal range?
Please reply. Less than.
How to detect the moisture content of sodium bicarbonate?
Direct weight loss on drying. What is the temperature at which trace water is titrated (or by the Coulometric method) with a Karl Fischer titrator?
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There are several ways to distinguish sodium carbonate from sodium bicarbonate:
1. Heating, sodium bicarbonate has poor thermal stability, and sodium bicarbonate can be decomposed.
2. Take the same amount of dissolved in water, and observe which of the two dissolves more, and the solubility of sodium bicarbonate is small.
3. Take the same amount of soluble in water, measure the car without its pH value, and the sodium carbonate is large.
4. Add hydrochloric acid dropwise, and hydrochloric acid dropwise added to sodium bicarbonate solution will immediately produce bubbles, while dropwise added to sodium carbonate solution will not produce bubbles. Extinction.
5. Add calcium chloride solution, use metathesis reaction, sodium carbonate solution reacts with calcium chloride to produce white precipitate, while sodium bicarbonate will not.
Sodium carbonate is commonly known as soda ash, soda, white powder, good thermal stability, and is not easy to decompose when heated.
Sodium bicarbonate, commonly known as baking soda, is a small white crystal, with poor thermal stability, and is easy to be separated and dissolved by heating.
Go to a certain sample.
After dissolving, excess hydrochloric acid is added to collect the gas produced to calculate the mol amount. >>>More
Known: ka1=, ka2=, sodium bicarbonate for carbonic acid.
pH = , RT, 25° then KW = 10 -14 then you can find KB1 = KW Ka2 , KB2 = KW KA1 According to the calculation of multiple weak bases, the sodium bicarbonate concentration of pH = is deduced from sodium bicarbonate PH=>PH= is relatively close, and it is calculated according to the substitution for comparison, KB2 * C is close to KB2 * 20 kW, so KB2 * C >> KB1 KB2 >100, and c kb1 is close, so c kb1 > 500 To sum up: kb2 * c >>20 kw, kb1 kb2>100, c kb1 > 500, meet the requirements of the simplified formula so, [oh-] 0 5 = kb1 * c seems to be wrong You take a look first The method is almost like this, first compare kb2 * c >>20 kw, kb1 kb2>100, c kb1 > 500 >>>More
2.Preparation method:
1) Laboratory method: >>>More
Sodium carbonate (soda ash) The chemical formula is Na2CO3, commonly known as soda ash, also known as soda and soda ash, an important chemical basic raw material, and the main product of the soda ash industry. It is usually a white powder, easy to decompose at high temperatures, soluble in water, and the aqueous solution is alkaline. Soda ash will deliquescent in humid air, slowly absorb carbon dioxide and water, and partially become sodium bicarbonate, so the packaging should be strict, otherwise it will absorb moisture and agglomerate, sodium carbonate and water will form Na2CO3·10H2O, Na2CO3·7H2O, Na2CO3·H2O three kinds of hydrates, of which Na2CO3·10H2O is the most stable, and the heat of dissolution soluble in water is very small. >>>More
The difference in their thermal stability allows the two substances to be identified. >>>More